2,4,6-三氨基-3,5-二硝基吡啶-1-氧化物,2,4,6-triamino-3,5-dinitropyridine-1-oxide英语短句,例句大全

2,4,6-三氨基-3,5-二硝基吡啶-1-氧化物,2,4,6-triamino-3,5-dinitropyridine-1-oxide
1)2,4,6-triamino-3,5-dinitropyridine-1-oxide2,4,6-三氨基-3,5-二硝基吡啶-1-氧化物
1.The results show that the best conditions are:DMSO as solvent and bubbling NH3 into the solution,the yield of the 2,4,6-triamino-3,5-dinitropyridine-1-oxide was up to 80%,and the content of 2,6-diamino-3,5-dinitropyridine-1-oxide was decrease to 0.结果表明,以DMSO为溶剂、反应过程中不断通入氨气,胺化反应的收率和选择性最佳,2,4,6-三氨基-3,5-二硝基吡啶-1-氧化物的收率可达到80%,副产物2,6-二氨基-3,5-二硝基吡啶-1-氧化物的收率降低至0。
2)2,6-diamino-3,5-dinitropyridine-1-oxide(ANPyO)2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)
1.In order to study the properties of 2,6-diamino-3,5-dinitropyridine-1-oxide(ANPyO),the three refined samples of ANPyO were prepared by recrystallization from the solvents of trifluoroacetic acid(CF3COOH),dimethyl sulfoxide(DMSO) and N,N-dimethyl formamide(DMF) respectively,and the properties of the three samples were compared.为了研究不同溶剂精制的2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)的性能,分别以三氟乙酸(CF3COOH)、二甲基亚砜(DMSO)和N,N-二甲基甲酰胺(DMF)为溶剂,采用重结晶法精制ANPyO,对精制后样品性能进行比较研究。
2.2,6-Diamino-3,5-dinitropyridine(ANPy) and 2,6-diamino-3,5-dinitropyridine-1-oxide(ANPyO) was reacted with aqueous ammonia and KMnO4 under different conditions.以氨水为胺化剂,KMnO4为氧化剂,在不同反应条件下实现2,6-二氨基-3,5-二硝基吡啶(ANPy)和2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)4位的氧化胺化反应,目标化合物2,4,6-三氨基-3,5-二硝基吡啶(TANPy)和2,4,6-三氨基-3,5-二硝基吡啶-1-氧化物(TANPyO)的收率分别达到81。
3)2,6-diamino-3,5-dinitropyridine-1-oxide2,6-二氨基-3,5-二硝基吡啶-1-氧化物
1.A novel synthetic method of 2,6-diamino-3,5-dinitropyridine-1-oxide (ANPyO) was explored using 2,6-diaminopyridine as the starting materials in three steps, including acetylation, N-oxidation and ni- tration.研究了2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)的合成新方法。
2.The results show that the best conditions are:DMSO as solvent and bubbling NH3 into the solution,the yield of the 2,4,6-triamino-3,5-dinitropyridine-1-oxide was up to 80%,and the content of 2,6-diamino-3,5-dinitropyridine-1-oxide was decrease to 0.结果表明,以DMSO为溶剂、反应过程中不断通入氨气,胺化反应的收率和选择性最佳,2,4,6-三氨基-3,5-二硝基吡啶-1-氧化物的收率可达到80%,副产物2,6-二氨基-3,5-二硝基吡啶-1-氧化物的收率降低至0。
3.A simple synthetic method of 2,6-diamino-3,5-dinitropyridine-1-oxide(DADNP-1-O) was de-scribed.研究了2,6-二氨基-3,5-二硝基吡啶-1-氧化物(DADNP-1-O)的一个简易合成方法。
4)2-amino-3,5-dinitropyridine-1-oxide2-氨基-3,5-二硝基吡啶-1-氧化物
1.Oxidative amination of 2-amino-3,5-dinitropyridine-1-oxide was studied with aqueous ammonia as amination agents and KMnO4 as oxidant under different conditions.用氨水作胺化剂、KMnO4作氧化剂,研究了不同反应条件下2-氨基-3,5-二硝基吡啶-1-氧化物的氧化胺化反应,讨论了氧化胺化反应机理以及溶剂、氨水浓度等对胺化产物收率和组成的影响。

英文短句/例句

1.Oxidative Amination of 2-Amino-3,5-dinitropyridine-1-oxide2-氨基-3,5-二硝基吡啶-1-氧化物的氧化胺化反应
2.Synthesis of 2,6-Diamino-3,5-dinitropyridine-1-oxide2,6-二氨基-3,5-二硝基吡啶-1-氧化物的合成新方法
3.Refining and Properties of 2,6-Diamino-3,5-dinitropyridine-1-oxide2,6-二氨基-3,5-二硝基吡啶-1-氧化物的精制及其性能研究
4.Effect of Coating on Some Properties of a New Explosive 2,6-Diamino-3,5-dinitropyridine-1-oxide包覆对新型炸药2,6-二氨基-3,5-二硝基吡啶-1-氧化物某些性能的影响
5.A Simple Method for Preparing 2,6-Diamino-3,5-dinitropyridine-1-oxide一个简易的2,6-二氨基-3,5-二硝基吡啶-1-氧化物的合成方法
6.Thermal Decomposition Kinetics of 2,6-Diamino-3,5-dinitropyridine 1-oxide and Its Formulation Explosives2,6-二氨基-3,5-二硝基吡啶-1-氧化物及其黏结炸药的热分解动力学
7.Oxidative Amination Reaction of 2,6-Diamino-3,5-dinitropyridine and its N-oxide2,6-二氨基-3,5-二硝基吡啶及其氮氧化物的氧化胺化反应
8.Preparation and Characterization of 2,6-Diamino-3,5-dinitropyridine (DADNP)2,6-二氨基-3,5-二硝基吡啶的制备及表征
9.Synthesis of 2-amino-6-methoxy-3-nitropyridine by Oxidative Amination氧化胺化反应合成2-氨基-6-甲氧基-3-硝基吡啶
10.The Crystal Structure of 3,5-di-Br-PADAT5-[(3,5-二溴-2-吡啶)偶氮]-2,4-二氨基甲苯的晶体结构
11.Dinitration of 2,6-Diamino(4-amino)pyridines2,6-二氨基(4-氨基)吡啶的二硝化反应
12.Synthesis and Characterization of 4-Amino-3,5-dinitropyrazole(LLM-116) Condensation Products4-氨基-3,5-二硝基吡唑(LLM-116)缩合物的合成与表征
13.Spectrophotometric Determination of Micro Amounts of Nickel With 2-[2-(3,5-Dibromopyridyl)Azo)-5-Di-ethylaminobenzoic Acid2-〔(3,5-二溴-2-吡啶)偶氮〕-5-二乙氨基苯甲酸分光光度法测定微量镍
14.Simultaneous spectrophotometric determination of Rhodium(Ⅲ) and Palladium(Ⅱ) with 2-(3,5-Dichloro-2-pyridylzao)-5-dimethylaminoaniline2-(3,5-二氯-2-吡啶偶氮)-5-二甲氨基苯胺光度法同时测定铑与钯
15.Synthesis of pyridin-ylmethyl 3,5-bis(pyridin-ylmethoxy)benzoate3,5-二(吡啶-甲氧基)苯甲酸吡啶-甲基酯的合成
16.Synthesis of 2- Amino-3-nitropyridine-6-methoxy2-氨基-3-硝基-6-甲氧基吡啶的合成研究
17.Synthesis of 3,5-Bis(pyridinylmethoxy)-benzoic Acid3,5-二(吡啶甲氧基)苯甲酸的合成
18.Synthesis of 2-chloro-5-nitropyridine and 4-amino-2-chloropyridine2-氯-5-硝基吡啶和4-氨基-2-氯吡啶的合成研究

相关短句/例句

2,6-diamino-3,5-dinitropyridine-1-oxide(ANPyO)2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)
1.In order to study the properties of 2,6-diamino-3,5-dinitropyridine-1-oxide(ANPyO),the three refined samples of ANPyO were prepared by recrystallization from the solvents of trifluoroacetic acid(CF3COOH),dimethyl sulfoxide(DMSO) and N,N-dimethyl formamide(DMF) respectively,and the properties of the three samples were compared.为了研究不同溶剂精制的2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)的性能,分别以三氟乙酸(CF3COOH)、二甲基亚砜(DMSO)和N,N-二甲基甲酰胺(DMF)为溶剂,采用重结晶法精制ANPyO,对精制后样品性能进行比较研究。
2.2,6-Diamino-3,5-dinitropyridine(ANPy) and 2,6-diamino-3,5-dinitropyridine-1-oxide(ANPyO) was reacted with aqueous ammonia and KMnO4 under different conditions.以氨水为胺化剂,KMnO4为氧化剂,在不同反应条件下实现2,6-二氨基-3,5-二硝基吡啶(ANPy)和2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)4位的氧化胺化反应,目标化合物2,4,6-三氨基-3,5-二硝基吡啶(TANPy)和2,4,6-三氨基-3,5-二硝基吡啶-1-氧化物(TANPyO)的收率分别达到81。
3)2,6-diamino-3,5-dinitropyridine-1-oxide2,6-二氨基-3,5-二硝基吡啶-1-氧化物
1.A novel synthetic method of 2,6-diamino-3,5-dinitropyridine-1-oxide (ANPyO) was explored using 2,6-diaminopyridine as the starting materials in three steps, including acetylation, N-oxidation and ni- tration.研究了2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)的合成新方法。
2.The results show that the best conditions are:DMSO as solvent and bubbling NH3 into the solution,the yield of the 2,4,6-triamino-3,5-dinitropyridine-1-oxide was up to 80%,and the content of 2,6-diamino-3,5-dinitropyridine-1-oxide was decrease to 0.结果表明,以DMSO为溶剂、反应过程中不断通入氨气,胺化反应的收率和选择性最佳,2,4,6-三氨基-3,5-二硝基吡啶-1-氧化物的收率可达到80%,副产物2,6-二氨基-3,5-二硝基吡啶-1-氧化物的收率降低至0。
3.A simple synthetic method of 2,6-diamino-3,5-dinitropyridine-1-oxide(DADNP-1-O) was de-scribed.研究了2,6-二氨基-3,5-二硝基吡啶-1-氧化物(DADNP-1-O)的一个简易合成方法。
4)2-amino-3,5-dinitropyridine-1-oxide2-氨基-3,5-二硝基吡啶-1-氧化物
1.Oxidative amination of 2-amino-3,5-dinitropyridine-1-oxide was studied with aqueous ammonia as amination agents and KMnO4 as oxidant under different conditions.用氨水作胺化剂、KMnO4作氧化剂,研究了不同反应条件下2-氨基-3,5-二硝基吡啶-1-氧化物的氧化胺化反应,讨论了氧化胺化反应机理以及溶剂、氨水浓度等对胺化产物收率和组成的影响。
5)2,6-diamino-3,5-dinitropyrazine-1-oxide2,6-二氨基-3,5-二硝基吡嗪-1-氧化物
1.A new synthetic method of 2,6-diamino-3,5-dinitropyrazine-1-oxide (LLM-105) was discribed.研究了2,6-二氨基-3,5-二硝基吡嗪-1-氧化物(LLM-105)的合成新方法。
6)3,5-dicyano-2,4,6-trimethylpyridine3,5-二氰基-2,4,6-三甲基吡啶
1.In this paper,3,5-dicyano-2,4,6-trimethylpyridine was prepared in high yield by photoinduced aromatization of 1,4-dihydro-3,5-dicyano-2,4,6-trimethylpyridine in CCl4 solution.3,5-二氰基-2,4,6-三甲基吡啶在新型光电功能材料的合成中有重要的应用价值。