%
[0196] V2-BB(2F，3F)_02 (2-4)9%
[0197] 1V2-BB(2F，3F)_04 (2-4)6%
[0198] V-HHB(2F，3F)_02 (2-6) 10%
[0199] V-HHB(2F，3F)_04 (2-6)3%
[0200] 1V2-HHB(2F，3F) -02 (2-6)4%
[0201] 3-HH10B(2F，3F)-02 (2-8) 11%
[0202] 3-HH-V (3-1)26%
[0203] 1-HH-2V1 (3-1)5%
[0204] 5-HB-02 (3-2)4%
[0205] 3-HHB-01 (3-5)5%
[0206] V-HHB-1 (3-5)4%
[0207] 制备介电各向异性为负的上述组合物，并测定特性。NI= 74. 0°C;Tc< -20°C; Δη= 0. 101 ；Δε= -3. 4；Vth= 2. 18V.
[0208] 在所述组合物中，以0. 3重量％的比例添加化合物（l-1-l-l)，以0. 1重量％的比 例添加化合物（4-2-3)。
[0209]
[0210] AC-V0-BB-0V-AC (4-2-3)
[0211] 进行紫外线照射而进行聚合后，测定响应时间。T = 4. 3ms.
[0212] [实施例3]
[0213] 3-BB(2F，3F)_02 (2-4)9%
[0214] 20-BB(2F，3F)_02 (2-4)3%
[0215] 2-HH10B(2F，3F)-02 (2-8) 10%
[0216] 3-HH10B(2F，3F)-02 (2-8)20%
[0217] 2-BB(2F，3F)B_4 (2-9)3%
[0218] 2-HH-3 (3-1) 19%
[0219] 3-HH-4 (3-1)4%
[0220] 3-HH-V (3-1)8%
[0221] V2-BB-1 (3-3)3%
[0222] l-BB-3 (3-3)6%
[0223] V-HHB-3 (3-5)5%
[0224] 3-HBB-2 (3-6)4%
[0225] 5-B (F) BB-2 (3-7)3%
[0226] 5-HBBH-3 (3-11)3%
[0227] 制备介电各向异性为负的上述组合物，并测定特性。NI = 83. 6°C ;Tc < -20°C ; Δη= 0. 108 ； Δε= -2.8；Vth= 2.34V.
[0228] 在所述组合物中，以0.2重量％的比例添加化合物（1-1-3-1)，以0.2重量％的比 例添加化合物（4-18-2)。
[0229]
[0230] MAC-BB (F) B-AC (4-18-2)
[0231] 进行紫外线照射而进行聚合后，测定响应时间。T = 3. 7ms.
[0232][实施例4]
[0233] 3-BB(2F，3F)_02 (2-4) 10%
[0234] 5-BB(2F，3F) -04 (2-4)3%
[0235] 2-HH10B(2F，3F)_02 (2-8) 10%
[0236] 3-HH10B(2F，3F)_02 (2-8)22%
[0237] 2-HH-3 (3-1)21%
[0238] 3-HH-V (3-1)8%
[0239] l-BB-3 (3-3)8%
[0240] 1V2-BB-1 (3-3)3%
[0241] V2-HHB-1 (3-5)5%
[0242] 3-HBB-2 (3-6)4%
[0243] 5-B(F)BB-3 (3-7)3%
[0244] 101-HBBH-4 (-)3%
[0245] 制备介电各向异性为负的上述组合物，并测定特性。NI= 78. 6°C;Tc< -20°C; Δη= 0. 107 ；Δε= -2. 6；Vth= 2. 39V.
[0246]在所述组合物中，以0. 2重量％的比例添加化合物（1-1-4-1)，以0. 2重量％的比 例添加化合物（4-1-1)。
[0247]
[0248] MAC-B(2F)B-MAC(4-1-1)
[0249] 进行紫外线照射而进行聚合后，测定响应时间。T=3. 8ms.
[0250][实施例5]
[0251] V2-BB(2F，3F)-02 (2-4) 12%
[0252] 1V2-BB(2F，3F)_02 (2-4)6%
[0253] 1V2-BB(2F，3F) -04 (2-4)3%
[0254] V-HHB(2F，3F) -01 (2-6)6%
[0255] V-HHB(2F，3F) -02 (2-6) 12%
[0256] V-HHB(2F，3F) -04 (2-6)5%
[0257] 3-HDhB(2F，3F)_02 (2-11)5%
[0258] 3-dhBB(2F，3F) -02 (2-14)4%
[0259] 3-HH-V (3-1)30%
[0260] l-BB-3 (3-3)6%
[0261] V-HHB-1 (3-5)5%
[0262] 1-BB(F)B_2V (3-8)3%
[0263] 3-HHEBH-4 (3-9)3%
[0264] 制备介电各向异性为负的上述组合物，并测定特性。NI = 77. 4°C ;Tc<-20°C; Δη= 0. 112 ；Δε= -2. 9；Vth= 2. 31V.
[0265]在所述组合物中，以0. 35重量％的比例添加化合物（1-1-5-1)，以0. 05重量％的 比例添加化合物（4-18-2)。
[0266]
[0267] MAC-BB (F) B-AC (4-18-2)
[0268] 进行紫外线照射而进行聚合后，测定响应时间。T = 4. 4ms.
[0269][实施例6]
[0270] V2-BB(2F，3F)_02 (2-4) 12%
[0271] 1V2-BB(2F，3F)_02 (2-4)6%
[0272] 1V2-BB(2F，3F)_04 (2-4)3%
[0273] V-HHB(2F，3F)-01 (2-6)6%
[0274] V-HHB (2F，3F) -02 (2-6)7%
[0275] V-HHB (2F，3F) -04 (2-6)5%
[0276] 1V2-HHB (2F，3F) -04 (2-6)5%
[0277] 3-HDhB(2F，3F)_02 (2-11)5%
[0278] 3-dhBB(2F，3F)_02 (2-14)5%
[0279] 3-HH-V (3-1)29%
[0280] V2-HB-1 (3-2)6%
[0281] V-HHB-1 (3-5)5%
[0282] 2-BB(F)B_5 (3-8)3%
[0283] 5-HBB(F)B_3 (3-13)3%
[0284] 制备介电各向异性为负的上述组合物，并测定特性。NI = 79. 0°C ;Tc < -20°C ; Δη=0.112 ； Δε= -2. 9 ；Vth = 2. 36V.
[0285] 在所述组合物中，以0.3重量％的比例添加化合物（1-1-6-1)，以0.1重量％的比 例添加化合物（4-18-1)。
[0286]
[0287] MAC-BB(F)B-0V-MAC (4-18-1)
[0288] 进行紫外线照射而进行聚合后，测定响应时间。T = 4. 4ms.
[0289][实施例7]
[0290] 3-HB(2F，3F)_02 (2-1)3%
[0291] V2-BB(2F，3F)_02 (2-4) 11%
[0292] 1V2-BB(2F，3F)_02 (2-4)6%
[0293] V2-HHB(2F，3F) -02 (2-6)5%
[0294] 3-HDhB(2F，3F)_02 (2-11)5%
[0295] 3-HBB(2F，3F)_02 (2-13)3%
[0296] V-HBB(2F，3F)_02 (2-13)6%
[0297] V2-HBB(2F，3F)_02 (2-13)6%
[0298] 3-dhBB(2F，3F)_02 (2-14)5%
[0299] 5-HH-01 (3-1)4%
[0300] 3-HH-V (3-1)25%
[0301] 3-HH-VFF (3-1)3%
[0302] l-BB-3 (3-3)6%
[0303] 3-HHEH-3 (3-4)3%
[0304] V-HHB-1 (3-5)6%
[0305] V2-HHB-1 (3-5)3%
[0306] 制备介电各向异性为负的上述组合物，并测定特性。NI = 75. 3°C ;Tc<-20°C; Δη= 0. 113 ； Δε= -2. 5 ；Vth = 2. 39V.
[0307] 在所述组合物中，以0.2重量％的比例添加化合物（l-1-l-l)，以0.1重量％的比 例添加化合物（4-2-4)。
[0308]
[0309] AC-V0-BB-MAC(4-2-4)
[0310] 进行紫外线照射而进行聚合后，测定响应时间。T=4. 5ms.
[0311][实施例8]
[0312] V2-BB(2F，3F)_02 (2-4) 10%
[0313] 1V2-BB(2F，3F)_02 (2-4)4%
[0314] 1V2-BB(2F，3F)_04 (2-4)4%
[0315] V-HHB(2F，3F)_01 (2-6)6%
[0316] V-HHB(2F，3F)_02 (2-6) 10%
[0317] V-HHB(2F，3F)_04 (2-6)5%
[0318] 3-DhH10B(2F，3F)-02 (2-12)3%
[0319] 3-HHB(2F，3CL)_02 (2-16)3%
[0320] 5-HBB(2F，3CL)_02 (2-17)3%
[0321] 3-H10Cro(7F，8F)-5 (2-18)3%
[0322] 3-HH10Cro(7F，8F)_5 (2-19)3%
[0323] 3-HH-V (3-1)29%
[0324] l-BB-3 (3-3)6%
[0325] V-HHB-1 (3-5)7%
[0326] 3-HBB-2 (3-6)4%
[0327] 制备介电各向异性为负的上述组合物，并测定特性。NI = 74. 5°C ;Tc < -20°C ; Δ η = 0. 105 ； Δ ε = -3. 0 ；Vth = 2. 22V.
[0328]在所述组合物中，以0. 25重量％的比例添加化合物（1-1-1-1)，以0. 05重量％的 比例添加化合物（4-2-3)。
[0329]
[0330] AC-V0-BB-0V-AC(4-2-3)
[0331] 进行紫外线照射而进行聚合后，测定响应时间。T = 4. 8ms.
[0332][实施例9]
[0333] V2-HB(2F，3F)_02 (2-1)5%
[0334] 3-H2B(2F，3F) -02 (2-2)9%
[0335] V-HHB(2F，3F) -02 (2-6) 12%
[0336] 2-HH10B(2F，3F)_02 (2-8)7%
[0337] 3-HH10B(2F，3F)_02 (2-8) 12%
[0338] 3-HDhB(2F，3F)_02 (2-11)3%
[0339] 2-HH-3 (3-1)27%
[0340] 3-HH-4 (3-1)4%
[0341] l-BB-3 (3-3)9%
[0342] 3-HHB-l (3-5)3%
[0343] 3-B (F) BB-2 (3-7)3%
[0344] 3-HB(F)HH_5 (3-10)3%
[0345] 3-HB(F)BH_3 (3-12)3%
[0346] 制备介电各向异性为负的上述组合物，并测定特性。NI = 79. 9°C ;Tc < -20°C ; Δ η = 0. 092 ； Δ ε = -2. 9 ；Vth = 2. 32V.
[0347]在所述组合物中，以0. 2重量％的比例添加化合物（1-1-3-1)，以0. 1重量％的比 例添加化合物（1-1-6-1)。
[0348]
[0349] 进行紫外线照射而进行聚合后，测定响应时间。T = 3. 9ms.
[0350][实施例 10]
[0351] 1V2-HB(2F，3F)_02 (2-1)5%
[0352] 5-H2B(2F，3F)_02 (2-2)9%
[0353] 5-HHB (2F，3F) -02 (2-6)3%
[0354] V-HHB (2F，3F) -02 (2-6)6%
[0355] 2-HH10B(2F，3F)-02 (2-8)7%
[0356] 3-HH10B(2F，3F)_02 (2-8) 12%
[0357] 2-BB(2F，3F)B_3 (2-9)3%
[0358] 2-HHB(2F，3CL)_02 (2-16)3%
[0359] 4-HHB(2F，3CL)_02 (2-16)3%
[0360] 2-HH-3 (3-1)22%
[0361] 3-HH-V (3-1)8%
[0362] l-BB-3 (3-3) 10%
[0363] 3-HHB-l (3-5)3%
[0364] 3-HB(F)HH_5 (3-10)3%
[0365] 3-HB(F)BH_3 (3-12)3%
[0366] 制备介电各向异性为负的上述组合物，并测定特性。NI = 80. 5°C ;Tc < -20°C ; Δη= 0.093 ；Δ ε =-2. 9 ；Vth=2. 32V.
[0367]在所述组合物中，以0. 1重量％的比例添加化合物（1-1-1-1)，以0. 3重量％的比 例添加化合物（1-1-3-1)。
[0368]
[0369] 进行紫外线照射而进行聚合后，测定响应时间。T= 4. 2ms.
[0370] [实施例 11]
[0371] 3-HB(2F，3F)_04 (2-1)5%
[0372]V-HB(2F，3F)_02 (2-1)4%
[0373] V2-BB(2F，3F)_02 (2-4)7%
[0374] 1V2-BB(2F，3F)_02 (2-4)6%
[0375] 20-B(2F，3F)B(2F，3F)-06 (2-5)3%
[0376] V-HHB(2F，3F) -02 (2-6) 10%
[0377] 3-HH2B(2F，3F)_02 (2-7)3%
[0378] 3-HH10B(2F，3F)_02 (2-8) 10%
[0379] 2-BB(2F，3F)B_3 (2-9)6%
[0380] 3-HH-V (3-1)27%
[0381] 4-HH-V1 (3-1)6%
[0382] 3-HH-2V1 (3-1)3%
[038